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The principle goal of this work is the grafting of polycaprolactone diol
(PCL) on the floor of oxidized nanocelluloses (ONC) in order to reinforce the compatibility
between the hydrophilic cellulose nanofibres and the hydrophobic polymer matrix.
This grafting was successfully realized with a brand new technique generally known as click
on chemistry. In this context, the oxidized nanocelluloses
bearing alkyl teams (ONC-PR) had been ready by reacting amino teams
of propargylamine (PR) with carboxyl groups of ONC.
In parallel, PCL was converted into azido-polycaprolactone (PCL-N3) in two steps: (i) tosylation of
polycaprolactone (PCL-OTs) and (ii) conversion of PCL-OTs into PCL-N3 by nucleophilic displacement using sodium azide.
Finally, ONC-PR was reacted with PCL-N3 in heterogeneous situations by
click chemistry so as to prepare polycaprolactone grafted oxidized nanocellulose (ONC-g-PCL), which may
very well be appropriate for improving the interfacial adhesion within the composite materials.
The grafted samples had been characterized by transmission electron microscopy and by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS) and Carbon-thirteen nuclear magnetic
resonance spectroscopy (13C-NMR) spectroscopic
techniques.
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